Dataset Authors

Dana Wetzel

Abstract

This dataset contains total polycyclic aromatic hydrocarbon (TPAH) concentrations of south Louisiana crude oil in sediment and tissue of field-collected red drum (Sciaenops ocellatus) and southern flounder (Paralichthys lethostigma) in the Gulf of Mexico from 2018-08-13 to 2018-08-16.

Comments

Supplemental Information

Sample Key: Collected Date (MM/DD/YYYY); Collected Location; Collected Time (hh:mm:ss); Field ID; MML; Matrix; Organism Species; Coordinates (degree N, degree W). Please note that column I (Fin Clip) in a worksheet "Sample Key" is a redundant field note and can be ignored. Liver Results: Species; Location, MML; Field ID; PAH Analytes; MDL (ng/g ww); ΣPAH (ng/g ww) Sediment Results: Location, MML; Field ID; PAH Analytes; MDL (ng/g); ΣPAH (ng/g) % Lipid: MML; Field ID; Matrix; % Lipid; Species Note: MML= Mote Marine Laboratory and MDL= Minimum Detectable Limit Nomenclature for sample IDs example: "CII-15-0000" means "Three-letter laboratory project code(CII=CIMAGE-II)-two digit year(2015=15)-four digit integral assigned by laboratory beginning at 0000 for each new year(0000 through 9999)".|Tissue samples were surrogated with naphthalene d8, acenaphthene d10, phenanthrene-d10, chrysene-d12, perylene d12 and extracted via EPA method 3545 using a Dionex ASE300, then concentrated to 10ml in DCM for analysis. Water samples were surrogated with naphthalene d8, acenaphthene d10, phenanthrene-d10, chrysene-d12, perylene d12 and extracted via EPA method 3510, and concentrated to 1mL in DCM for analysis. PAHs were analyzed using gas chromatography/mass spectrometry in selected ion monitoring mode using a 0.25 um film thickness, 0.25 mm I.D., and 30 m length capillary column. One microliter of the sample was injected at 60ºC, held for 1.5 minutes. The temperature was then increased to 325 ºC at a rate of 8 ºC/ min and held for 3 min.|Dionex ASE300 Accelerated Solvent Extractor, Agilent 7890A/5975C, Zebron Capillary column.||Average surrogate recovery 50-150. CCV run before and after every ten samples. CCV passing recovery must be average less than 20%. CCV means Continued Calibration Verification.|

Purpose

Field study to evaluate the TPAH concentrations of south Louisiana crude oil in sediment and tissue of field collected red drum and southern flounder.

Keywords

Deepwater Horizon, Flounder, sediment, red drum, total polycyclic aromatic hydrocarbon, Sciaenops ocellatus, Paralichthys lethostigma, TPAH

UDI

R6.x805.000:0034

Date

September 2019

Point of Contact

Name

Dana Wetzel

Organization

Mote Marine Laboratory / Environmental Laboratory of Forensics Program

Funding Source

RFP-6

DOI

10.7266/n7-75ct-5274

Rights Information

Creative Commons License
This work is licensed under a Creative Commons Public Domain Dedication 1.0 License.

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